HRID390063

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6422

未命名化合物

结构：CSc1nc(Nc2cccc(C)c2)c2c(=O)[nH]cc(Br)c2n1

HCID58296328

未命名化合物

结构：CC(C)(C)OC(=O)NCCCN.O=C(OO)c1cccc(Cl)c1

HCID86654203

未命名化合物

PRODUCTS

生成物

结构：Cc1cccc(Nc2nc(NCCCN)nc3c(Br)c[nH]c(=O)c23)c1

HCID44818367

未命名化合物

PROCEDURE

实验过程

The product was prepared from 8-bromo-4-[(3-methylphenyl)amino]-2-(methylthio)pyrido[4,3-d]pyrimidin-5(6H)-one using mCPBA/1,1-dimethylethyl (3-aminopropyl)carbamate and TFA sequences similar that described for Example 1 (Scheme 2). It was purified using reverse-phase HPLC.

WORKUP

后处理

customIt was purified