HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 58295791, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 58295703 | HCID 58295703 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 58295791 | HCID 58295791 | — |
Reaction Steps
The title compound was prepared following a procedure analogous to that described in Example 7 using 0.5 M NH3 in dioxane and (±)-(E)-2-(6-fluoro-1′-(3-(2-(trifluoromethyl)phenyl)acryloyl)-2,3-dihydrospiro[indene-1,4′-piperidine]-3-yl)acetic acid. LC-MS Method 1 tR=1.67, min, m/z=461.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383629B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-b62efa0a040a497186686003e86c701d |
| Source note | uspto-grants-2013_02 |