HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanogen Bromide → HCID 58625098, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanogen Bromide | HCID 10476 | — |
| Reactant | HCID 58625144 | HCID 58625144 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 58625098 | HCID 58625098 | — |
Reaction Steps
Cyanogen bromide (0.00034 mol) was added to a mixture of N-[2-(4′-amino-3′-propylaminomethyl-biphenyl-2-yl)-ethyl]-benzenesulfonamide (0.00031 mol) in ethanol (1 mL) in a Fast-tube, and then the reaction mixture was stirred overnight at room temperature. The solvent was evaporated and the residue was purified by high-performance liquid chromatography. The purest product fractions were collected and the solvent was evaporated to yield the title compound as a residue.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383637B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-4ed908823dd440dab22600e1c982701b |
| Source note | uspto-grants-2013_02 |