HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67322618, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67323585 | HCID 67323585 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67322618 | HCID 67322618 | — |
Reaction Steps
A solution of tert-butyl 4-fluoro-4-pyridin-2-ylpiperidine-1-carboxylate (0.075 g, 0.27 mmol.) in 10 mL of ethyl acetate was saturated with gaseous HCl. After 1 h, the reaction was concentrated in vacuo to provide 2-(4-fluoropiperidin-4-yl)pyridine that gave a mass ion (ES+) of 181.1 for [M+H]+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383638B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-ae02786b5a4a4d619b8c3ad96cdc256a |
| Source note | uspto-grants-2013_02 |