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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 390416Generated: October 29, 2026

Cesium carbonate → HCID 58066681, compound

https://huagongshe.com/reaction/390416

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCesium carbonateHCID 10796—
Reactant2-(1H-Pyrazol-4-yl)acetonitrileHCID 20542700—
ReactantHCID 58066671HCID 58066671—
SolventAcetonitrileHCID 6342—
ProductHCID 58066681HCID 58066681—

Reaction Steps

(1H-Pyrazol-4-yl)-acetonitrile (0.19 g, 1.77 mmol) and N-(4-bromomethyl-3-tert-butylsulfanylmethyl-phenyl)-2,2-dimethyl-propionamide (0.20 g, 0.55 mmol) were combined in MeCN. Cesium carbonate (0.95 g, 2.90 mmol) was added, and the reaction was stirred for 45 minutes at room temperature. The mixture was worked-up and purified by silica gel chromatography to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08383654B2
Source datasetuspto-grants-2013_02
ORD IDord-5d951142a32340fa98a32ed337862b90
Source noteuspto-grants-2013_02