HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Cyanide → HCID 58066678, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Cyanide | HCID 9032 | — |
| Reactant | HCID 58066671 | HCID 58066671 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 58066678 | HCID 58066678 | — |
Reaction Steps
N-(4-Bromomethyl-3-tert-butylsulfanylmethyl-phenyl)-2,2-dimethyl-propionamide (1.8 g, 4.8 mmol) in DMSO (40 mL) was treated with potassium cyanide (0.325 g, 5.0 mmol), and the reaction was stirred for 1 hour at room temperature. The mixture was worked-up and purified by silica gel chromatography to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383654B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-8d0eb7a24e1945c1adeb85fb98b65fbe |
| Source note | uspto-grants-2013_02 |