Ammonia → HCID 69004301, compound

Participants

Reaction Steps

The titled compound was prepared as the hydrochloride salt according to Method CB using the product of Example 18B (91 mg, 0.5 mmol) and 3-ethynylpyridine (Aldrich, 52 mg, 0.5 mmol). 1H NMR (300 MHz, DMSO-d6) δ 7.64 (dd, J=7.5, 4.4 Hz, 1H), 7.80 (t, J=7.5 Hz, 1H), 7.89 (s, 1H), 8.04 (dt, J=7.7, 1.3 Hz, 1H), 8.21-8.34 (m, 2H), 8.38 (t, J=1.4 Hz, 1H), 8.74 (dd, J=4.8, 1.6 Hz, 1H), 9.13 (d, J=2.0 Hz, 1H) ppm; MS (DCI/NH3) m/z 248 (M+H)+.

Provenance & Evidence