Ammonia → HCID 928838, compound

Participants

Reaction Steps

The titled compound was prepared according to Method CB using the product of Example 1A (78 mg, 0.5 mmol) and 1-ethynyl-benzene (Aldrich, 52 mg, 0.5 mmol). 1H NMR (300 MHz, MeOH-d4) δ 7.37 (s, 1H), 7.46-7.68 (m, 4H), 7.85-8.00 (m, 2H), 8.37 (dt, J=7.9, 2.0 Hz, 1H), 8.66 (dd, J=4.9, 1.5 Hz, 1H), 9.10 (d, J=2.4 Hz, 1H) ppm; MS (DCI/NH3) m/z 223 (M+H)+.

Provenance & Evidence