Ammonia → HCID 44546414, compound

Participants

Reaction Steps

The titled compound was prepared as the trifluoroacetic acid salt according to Method CD using the product of Example 28B (88 mg, 0.5 mmol) and 3-ethynylaniline (Aldrich, 59 mg, 0.5 mmol). 1H NMR (300 MHz, MeOH-d4) δ 6.82-6.91 (m, 1H), 7.13-7.49 (m, 4H), 8.16 (dt, J=9.2, 2.2 Hz, 1H), 8.60 (d, J=2.7 Hz, 1 H), 8.96 (s, 1H) ppm; MS (DCI/NH3) m/z 256 (M+H)+.

Provenance & Evidence