HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 44546487, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3-Methylphenylacetylene | HCID 136600 | — |
| Reactant | N-Hydroxypyrimidine-5-carbimidoyl chloride | HCID 86636847 | — |
| Product | HCID 44546487 | HCID 44546487 | — |
Reaction Steps
The titled compound was prepared as the hydrochloride salt according to Method CB using the product of Example 44B (79 mg, 0.5 mmol) and 1-ethynyl-3-methylbenzene (Aldrich, 58 mg, 0.5 mmol). 1H NMR (300 MHz, DMSO-d6) δ 2.42 (s, 3H), 7.39 (d, J=7.8 Hz, 1H), 7.49 (t, J=7.8 Hz, 1H), 7.67-7.79 (m, 3H), 9.33 (s, 2 H), 9.35 (s, 1H) ppm; MS (DCI/NH3) m/z 238 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383658B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-b80b315afcb44caa987b5f543b266bf0 |
| Source note | uspto-grants-2013_02 |