HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 44546541, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 86140908 | HCID 86140908 | — |
| Reactant | 5-Fluoro-N-hydroxynicotinimidoyl chloride | HCID 86636846 | — |
| Product | HCID 44546541 | HCID 44546541 | — |
Reaction Steps
The titled compound was prepared according to Method CB using the product of product of Example 28B (88 mg, 0.5 mmol) and product of Example 60A (76 mg, 0.5 mmol). 1H NMR (300 MHz, MeOH-d4) 87.71 (s, 1H), 8.15 (d, J=8.8 Hz, 1H), 8.19 (ddd, J=9.2, 2.7, 1.7 Hz, 1H), 8.37 (dd, J=8.2, 2.7 Hz, 1H), 8.55 (d, J=1.4 Hz, 1H), 8.63 (d, J=2.7 Hz, 1H), 8.98 (t, J=1.5 Hz, 1H) ppm; MS (DCI/NH3) m/z 291 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383658B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-082510f21f2242649213fc5cdb68e0bb |
| Source note | uspto-grants-2013_02 |