Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Quinoline | HCID 7047 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | Quinoline methiodide | HCID 19848 | — |
Reaction Steps
N-methylquinolinium iodide (Compound III) was synthesized according to the description in the aforementioned reference. Specifically, 2.4 mL of quinoline and 4 mL of methyl iodide were added to 42 mL of anhydrous dioxane, which was stirred at 150° C. for one hour. Thereafter, it was filtered and thereby a precipitate was collected and then washed with ether and petroleum ether. This was dried and thus N-methylquinolinium iodide (Compound III) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08383792B2 |
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| Source dataset | uspto-grants-2013_02 |
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| ORD ID | ord-6af5ef6efe2a4092938a0c01e49a2c54 |
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| Source note | uspto-grants-2013_02 |
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