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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 391163Generated: October 30, 2026

Methyl iodide → Quinoline methiodide

https://huagongshe.com/reaction/391163

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantQuinolineHCID 7047—
Solvent1,4-DioxaneHCID 31275—
ProductQuinoline methiodideHCID 19848—

Reaction Conditions

Temperature150 °C

Reaction Steps

N-methylquinolinium iodide (Compound III) was synthesized according to the description in the aforementioned reference. Specifically, 2.4 mL of quinoline and 4 mL of methyl iodide were added to 42 mL of anhydrous dioxane, which was stirred at 150° C. for one hour. Thereafter, it was filtered and thereby a precipitate was collected and then washed with ether and petroleum ether. This was dried and thus N-methylquinolinium iodide (Compound III) was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08383792B2
Source datasetuspto-grants-2013_02
ORD IDord-6af5ef6efe2a4092938a0c01e49a2c54
Source noteuspto-grants-2013_02