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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 391577Generated: October 30, 2026

O-Methylhydroxylamine hydrochloride → HCID 57657837, compound

https://huagongshe.com/reaction/391577

Reaction equation

Participants

RoleNameHCIDCharge
ReactantO-Methylhydroxylamine hydrochlorideHCID 521874—
Reactant3-Ethynylbenzoic acidHCID 15897047—
ProductHCID 57657837HCID 57657837106.7%

Reaction Steps

In a manner similar to that described for Example 478 (step 1), 3-ethynylbenzoic acid (0.1 g, 0.685 mmol) and O-methylhydroxylamine hydrogen chloride (0.057 g, 0.685 mmol) were reacted to give the title compound (0.128 g, 61%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08383825B2
Source datasetuspto-grants-2013_02
ORD IDord-ec3158799be9404aa6d7eb59700f0935
Source noteuspto-grants-2013_02