O-Methylhydroxylamine hydrochloride → HCID 57657837, compound

HRID 391577Notes

Reaction equation

HRID 391577 reaction equation
[C:1]([C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][CH:11]=1)[C:6](O)=[O:7])#[CH:2].Cl.[CH3:13][O:14][NH2:15]>>[C:1]([C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][CH:11]=1)[C:6]([NH:15][O:14][CH3:13])=[O:7])#[CH:2]

Participants

3

Reactant 2

HCID 521874O-Methylhydroxylamine hydrochlorideHCID 158970473-Ethynylbenzoic acid

Product 1

HCID 57657837HCID 57657837, compoundYield 106.7%

Procedure

In a manner similar to that described for Example 478 (step 1), 3-ethynylbenzoic acid (0.1 g, 0.685 mmol) and O-methylhydroxylamine hydrogen chloride (0.057 g, 0.685 mmol) were reacted to give the title compound (0.128 g, 61%).

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-ec3158799be9404aa6d7eb59700f0935
Source dataset
uspto-grants-2013_02
Patent number
US08383825B2

Reaction notes

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