HRID391722

反应详情

EQUATION

反应方程式

HRID 391722 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

555 mg (1.11 mmol) of the compound from Example 7A are dissolved in 15 ml of THF, 150 mg of palladium on carbon are added and the mixture is hydrogenated in a hydrogen atmosphere at atmospheric pressure until the theoretical amount of hydrogen has been taken up. The catalyst is filtered off, which gives, after concentration under reduced pressure, 520 mg (99% of theory) of the title compound.

WORKUP

后处理

  1. filtrationThe catalyst is filtered off
  2. customwhich gives
  3. concentrationafter concentration under reduced pressure, 520 mg (99% of theory) of the title compound