HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 22663050, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 23521605 | HCID 23521605 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22663050 | HCID 22663050 | — |
Reaction Steps
A solution of t-Butyl [2-{1-(3-methoxybenzenesulfonyl)-1H-pyrrolo[2,3-c]pyridin-3-yl}-ethyl]carbamate in CH2Cl2 is treated with trifluoroacetic acid, stirred for 2 h and concentrated in vacuo. The resultant residue is purified by preparative reverse phase HPLC to afford the title-final product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06800640B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-6bb057a030fe4248a3edfb6b2f6ffaa3 |
| Source note | uspto-grants-2004_10 |