HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanesulfonyl chloride → N-(3-(2-phenylphenoxy)phenyl)-N-(ethylsulfonyl)pyrid-3-ylmethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanesulfonyl chloride | HCID 11667 | — |
| Reactant | N-(3-(2-phenylphenoxy)phenyl)pyrid-3-ylmethylamine | HCID 69881268 | — |
| Product | N-(3-(2-phenylphenoxy)phenyl)-N-(ethylsulfonyl)pyrid-3-ylmethylamine | HCID 23521680 | — |
Reaction Steps
Using the procedure of Example 342 using N-(3-(2-phenylphenoxy)phenyl)pyrid-3-ylmethylamine and ethanesulfonyl chloride (Aldrich) and purifying via preparative HPLC eluting with 99:1 to 97:3 DCM/MeOH gave the title compound. Anal Calcd for C26H24N2O3S: C, 70.25; H, 5.44; N, 6.30. Found: C, 70.13; H, 5.39; N, 6.26. MS found 445.1 [M+H]+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06800651B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-f772445d2f6b496ca4eda25d69213a44 |
| Source note | uspto-grants-2004_10 |