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HRID392414

反应详情

EQUATION

反应方程式

HRID 392414 的结构方程式

REACTANTS

反应物

2
结构：CCS(=O)(=O)Cl
HCID11667

Ethanesulfonyl chloride

C2H5ClO2S

结构：c1ccc(-c2ccccc2Oc2cccc(NCc3cccnc3)c2)cc1
HCID69881268

未命名化合物

PRODUCTS

生成物

1
结构：CCS(=O)(=O)N(Cc1cccnc1)c1cccc(Oc2ccccc2-c2ccccc2)c1
HCID23521680

未命名化合物

PROCEDURE

实验过程

Using the procedure of Example 342 using N-(3-(2-phenylphenoxy)phenyl)pyrid-3-ylmethylamine and ethanesulfonyl chloride (Aldrich) and purifying via preparative HPLC eluting with 99:1 to 97:3 DCM/MeOH gave the title compound. Anal Calcd for C26H24N2O3S: C, 70.25; H, 5.44; N, 6.30. Found: C, 70.13; H, 5.39; N, 6.26. MS found 445.1 [M+H]+

WORKUP

后处理

  1. custompurifying via preparative HPLC
  2. washeluting with 99:1 to 97:3 DCM/MeOH