HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanesulfonyl chloride → HCID 23521728, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanesulfonyl chloride | HCID 11667 | — |
| Reactant | 4-bromo-N-(pyridin-3-ylmethyl)aniline | HCID 742774 | — |
| Product | HCID 23521728 | HCID 23521728 | — |
Reaction Steps
Using the procedure of Example 343 using N-(4-bromophenyl)pyridin-3-ylmethylamine and ethanesulfonyl chloride (Aldrich) and purifying via preparative HPLC eluting with 90:10 to 70:30 DCM/ethyl acetate gave the title compound. Anal Calcd for C14H15BrN2O2S: C, 47.33; H, 4.26; N, 7.88. Found: C, 47.24; H, 4.23; N, 7.79. MS found 354.0, 355.9 FD.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06800651B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-71b8add32e49412b82d877158351fa65 |
| Source note | uspto-grants-2004_10 |