HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluorophenol → HCID 69880868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluorophenol | HCID 9707 | — |
| Reactant | 4-bromo-N-(pyridin-3-ylmethyl)aniline | HCID 742774 | — |
| Product | HCID 69880868 | HCID 69880868 | — |
Reaction Steps
Using the method of Example 342 using N-(4-bromophenyl)pyridin-3-ylmethylamine and 2-fluorophenol (Aldrich)and purifying via preparative HPLC eluting with 90:10 to 80:20 DCM/ethyl acetate gave N-(4-(2-fluorophenoxy)phenyl)pyrid-3-ylmethylamine. Anal Calcd for C18H15FN2O: C, 73.45; H, 5.14; N, 9.52. Found: C, 73.36; H, 5.22; N, 9.35. MS found 295.1 [M+H]+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06800651B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-25cfcd47a3e3473093357d9d679fd19e |
| Source note | uspto-grants-2004_10 |