HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 39247Generated: October 28, 2026
Sulfuryl chloride → HCID 86762023, compound
https://huagongshe.com/reaction/39247
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | S-Ethyl O-1-(4,4-bis(diethylphosphono)butanoyloxy)ethyl carbonothioate | HCID 86762024 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86762023 | HCID 86762023 | — |
Reaction Steps
Sulfuryl chloride (78 μL, 0.96 mmol) was added drop-wise to a solution of 23 (237 mg, 0.48 mmol) in 10 mL of CH2Cl2 cooled to 0° C. The solution was stirred for 2 h. The solvent was removed under reduced pressure to afford chloroformate 24 and which was used for the next reaction without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08524691B2 |
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| Source dataset | uspto-grants-2013_09 |
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| ORD ID | ord-6e28a8d386fe456a9190bdf5a12e38f0 |
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| Source note | uspto-grants-2013_09 |
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