HRID392480
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
The compound was prepared as described in Example 3 by adding 3,5-dimethoxy-4-hydroxycinnamaldehyde (0.1 g, 0.48 mmol) to 2-cyanoacetamide (0.04 g, 0.48 mmol). After refluxing for 3 h and recrystallization from ethanol an orange solid was obtained (0.083 g, 63%). The product gave the following analytical data:
WORKUP
后处理
- customThe compound was prepared
- temperatureAfter refluxing for 3 h
- customrecrystallization from ethanol an orange solid
- customwas obtained (0.083 g, 63%)
- customThe product gave the following analytical data