HRID392480

反应详情

EQUATION

反应方程式

HRID 392480 的结构方程式

PROCEDURE

实验过程

The compound was prepared as described in Example 3 by adding 3,5-dimethoxy-4-hydroxycinnamaldehyde (0.1 g, 0.48 mmol) to 2-cyanoacetamide (0.04 g, 0.48 mmol). After refluxing for 3 h and recrystallization from ethanol an orange solid was obtained (0.083 g, 63%). The product gave the following analytical data:

WORKUP

后处理

  1. customThe compound was prepared
  2. temperatureAfter refluxing for 3 h
  3. customrecrystallization from ethanol an orange solid
  4. customwas obtained (0.083 g, 63%)
  5. customThe product gave the following analytical data