HRID392484

反应详情

EQUATION

反应方程式

HRID 392484 的结构方程式

PROCEDURE

实验过程

The compound was prepared as described in Example 3 by adding 4-nitrocinnamaldehyde (0.051 g, 0.29 mmol) to 2-amino-1-propene-1,1,3-tricarbonitrile (0.038 g, 0.29 mmol). After refluxing for 4 h and recrystallization from ethanol a yellow solid was obtained (0.08 g, 51%). The product gave the following analytical data:

WORKUP

后处理

  1. customThe compound was prepared
  2. temperatureAfter refluxing for 4 h
  3. customrecrystallization from ethanol a yellow solid
  4. customwas obtained (0.08 g, 51%)
  5. customThe product gave the following analytical data