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2-Amino-1-propene-1,1,3-tricarbonitrile → (E,E)-2-(1-Amino-2,2-dicyanoethenyl)-3-(4-nitrostyryl)acrylonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-1-propene-1,1,3-tricarbonitrile | HCID 13356 | — |
| 反応物 | 3-(4-Nitrophenyl)prop-2-enal | HCID 15614 | — |
| 生成物 | (E,E)-2-(1-Amino-2,2-dicyanoethenyl)-3-(4-nitrostyryl)acrylonitrile | HCID 86588371 | — |
反応手順
The compound was prepared as described in Example 3 by adding 4-nitrocinnamaldehyde (0.051 g, 0.29 mmol) to 2-amino-1-propene-1,1,3-tricarbonitrile (0.038 g, 0.29 mmol). After refluxing for 4 h and recrystallization from ethanol a yellow solid was obtained (0.08 g, 51%). The product gave the following analytical data:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06800659B2 |
| 出典データセット | uspto-grants-2004_10 |
| ORD ID | ord-f7bdd87b05274d70a960490cd9a1527e |
| 出典メモ | uspto-grants-2004_10 |