HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18712878, compound → HCID 22662897, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18712878 | HCID 18712878 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22662897 | HCID 22662897 | 66.8% |
Reaction Steps
A mixture of the title compound(1.7 g) from Step D and Pd(OH)2 on carbon (0.2 g) in EtOH (20 mL) was stirred at 50 psi under an atmosphere of hydrogen for 24 h. The catalyst was filtered to give the title compound (0.508 g, 66.8%). m/z=137 (MH+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06800636B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-16a2622ff0c34445ae12248849541ea1 |
| Source note | uspto-grants-2004_10 |