HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl 4-(1H-imidazol-1-yl)piperidine-1-carboxylate → 4-(1H-Imidazol-1-yl)piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl 4-(1H-imidazol-1-yl)piperidine-1-carboxylate | HCID 22662911 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 4-(1H-Imidazol-1-yl)piperidine | HCID 15789922 | — |
Reaction Steps
The title compound(0.21 g, 0.836 mmoles) from Step C was stirred in 4N HCl in dioxane (5 mL) for 2 h and then evaporated to dryness to give the title compound which was used to couple with the tricylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06800636B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-0afdb07d357e41c5bcf1446b96ce83bb |
| Source note | uspto-grants-2004_10 |