Hydracrylonitrile → HCID 54341459, compound

HRID 392697Notes

Reaction equation

[C:1]1([CH:7]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[C:8]([N:10]=[C:11]=[O:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH:19][CH2:20][CH2:21][C:22]#[N:23]>>[C:22]([CH2:21][CH2:20][O:19][C:11](=[O:12])[NH:10][C:8](=[O:9])[CH:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)#[N:23]

Participants

Reactant 2

HCID 8011Hydracrylonitrile

HCID 11264874Diphenylacetyl isocyanate

Product 1

HCID 54341459HCID 54341459, compound

Procedure

The title compound, white solid, m.p. 113° C. and MS:.m/e=308.3 (M+H+) was prepared in accordance with the general method of example 1 from diphenylacetyl isocyanate and 3-hydroxy-propionitrile.

Sources & evidence

ORD record: ord-858d2939323a4daeb034540567a04c4b
Source dataset: uspto-grants-2004_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06803381B1

Reaction notes

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