HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-Ethyl-1,3,4-oxadiazol-2-amine → N-(5-Ethyl-[1,3,4]oxadiazol-2-yl)-2,2-diphenyl-acetamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-Ethyl-1,3,4-oxadiazol-2-amine | HCID 343487 | — |
| Edukt | 1-(3,5-Dimethylpyrazol-1-yl)-2,2-diphenylethanone | HCID 774398 | — |
| Produkt | N-(5-Ethyl-[1,3,4]oxadiazol-2-yl)-2,2-diphenyl-acetamide | HCID 22661073 | — |
Reaktionsschritte
The title compound, white solid, m.p. 123-125° C. and MS: m/e=308.2 (M+H+) was prepared in accordance with the general method of example 48a from l-(3,5-dimethyl-pyrazol-1-yl)-2,2-diphenyl-ethanone and 5-ethyl-[1,3,4]oxadiazol-2-ylamine. The 1-(3,5-dimethyl-pyrazol-1-yl)-2,2-diphenyl-ethanone, white solid, m.p. 91-92° C. and MS: m/e=291.2 (M+H+) used in the above reaction was prepared in accordance with the general method of example 48c from 2,2-diphenylacetic acid hydrazide [Chem. Zentralblatt. 100, 2414(1929)] and acetylacetone.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06803381B1 |
| Quelldatensatz | uspto-grants-2004_10 |
| ORD ID | ord-039e57898f08497c9d15b3a70533b7d9 |
| Quellennotiz | uspto-grants-2004_10 |