1-Hexanol → HCID 22648628, compound

HRID 393137Notes

Reaction equation

[C:1]1([C:7](=[O:12])[C:8]([O:10][CH3:11])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:13](O)[CH2:14][CH2:15][CH2:16][CH2:17]C>>[C:1]1([C:7](=[O:12])[C:8]([O:10][CH2:11][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

Reactant 2

HCID 81031-Hexanol

HCID 84835Methyl phenylglyoxalate

Product 1

HCID 22648628HCID 22648628, compoundYield 87%

Procedure

16.42 g (0.1 mol) of methyl phenylglyoxalate is transesterified as described in example 1.1, using 1-hexanol instead of methoxyethanol. 21.33 g (87%) hexyl phenylglyoxalate are obtained as a colorless liquid.

Sources & evidence

ORD record: ord-811b43e5184f404e916b495f1de84d2c
Source dataset: uspto-grants-2004_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06806024B1

Reaction notes

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