HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178508255, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 178514143 | HCID 178514143 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178508255 | HCID 178508255 | — |
Reaction Steps
The product of step (a) (7.35 g) was heated at 120° C. in dimethylformamide (40 mL) and water (10 mL) for 10 hours. After cooling, the resulting solid was filtered off, washed with water, ether and ethyl acetate to give the title compound containing 0.4 moles of dimethylformamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06806273B1 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-1147a04203a9450d8f784dfb4bfdb789 |
| Source note | uspto-grants-2004_10 |