HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butyl nitrite → HCID 178447700, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butyl nitrite | HCID 10906 | — |
| Reactant | Bromotrimethylsilane | HCID 76113 | — |
| Reactant | HCID 178447701 | HCID 178447701 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178447700 | HCID 178447700 | — |
Reaction Steps
Trimethylsilyl bromide (0.44 mL) was added slowly to a solution at 0° C. under nitrogen of us t-butyl nitrite (0.42 mL) in acetonitrile (2 mL). After 30 minute at 0° C., 2-amino-5-(pentylthio)thiazolo[4,5-d]pyrimidin-7(4H)-one (0.5 g) (product of Example 10) was added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06806273B1 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-213296d7e40c43adb9c1fd56fb50261a |
| Source note | uspto-grants-2004_10 |