HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → p-(5-Octylpyridyl)benzoylchloride hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | p-(5-Octylpyridyl)benzoic acid | HCID 14070040 | — |
| Product | p-(5-Octylpyridyl)benzoylchloride hydrochloride | HCID 20153528 | 96.7% |
Reaction Steps
30 g (0.102 mol) of the resulting p-(5-octylpyridyl)benzoic acid was added to 24.3 g (0.204 mol) of thionyl chloride and reflux was maintained for 5 hours. The surplus thionyl chloride was removed by distillation and the product was recrystallized from hexane to obtain 34.5 g (0.0986 mol) of p-(5-octylpyridyl)benzoylchloride hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04723018 |
| Source dataset | uspto-grants-1988_02 |
| ORD ID | ord-c2ce3ae82b19475192f1d27047229762 |
| Source note | uspto-grants-1988_02 |