HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → Oxazol-5-ylmethyl 1H-imidazole-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | 1,3-Oxazol-5-ylmethanol | HCID 18758985 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Oxazol-5-ylmethyl 1H-imidazole-1-carboxylate | HCID 57443694 | — |
Reaction Steps
Oxazol-5-ylmethanol (0.15 g, 1.51 mmol) in anhydrous CH2Cl2 (5 mL) under a dry N2 atmosphere was treated with 1,1′-carbonyldiimidazole (0.20 g, 1.23 mmol) at ambient temperature and stirred for 2 hours to provide the title compound in a solution of CH2Cl2 which was used in subsequent Examples without further manipulation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08524753B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-f1427693f0e24c61b207944f53e8ebc9 |
| Source note | uspto-grants-2013_09 |