huagongshe.com
HRID393842

反应详情

EQUATION

反应方程式

HRID 393842 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)c1cc(C(=O)NCc2ccc([N+](=O)[O-])cc2)cc(C(C)(C)C)c1O
HCID21918554

未命名化合物

结构：O=C(NCCc1ccc([N+](=O)[O-])cc1)c1cc(O)c(O)c(O)c1
HCID21918749

未命名化合物

PRODUCTS

生成物

1
结构：Nc1ccc(CCNC(=O)c2cc(O)c(O)c(O)c2)cc1
HCID21918737

未命名化合物

收率 89%

PROCEDURE

实验过程

The experimental protocol used is the same as that described for intermediate 2.2, with 3,4,5-trihydroxy-N-[2-(4-nitrophenyl)ethyl]-benzamide replacing the 3,5-bis-(1,1-dimethylethyl)-4-hydroxy-N-[(4-nitrophenyl)methyl]-benzamide. A beige powder is obtained with a yield of 89%. Melting point: 167-169° C.

WORKUP

后处理

  1. customA beige powder is obtained with a yield of 89%