HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 15505948, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Chlorobenzene | HCID 7964 | — |
| Reactant | HCID 15505944 | HCID 15505944 | — |
| Reactant | Methylenechloride Hexane | HCID 21226440 | — |
| Product | HCID 15505948 | HCID 15505948 | — |
Reaction Steps
The synthesis was carried out essentially as described for 2a, but chlorobenzene was used as a solvent instead of methylene chloride. Yield after column chromatography (methylene chloride/ hexane): 48%. Found: C, 85.52; H, 4.21; C33H20O3 (NM 464.51) requires C, 85.33; H, 4.34%. Mass-spectrum, MALDI-TOF: 464.22 (100), 300.1 (30). Calculated exact mass for C33H20O3:464.14125; found 464.14189 [1.4 ppm error].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06809220B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-392d598f54414c4daad1f435d1438149 |
| Source note | uspto-grants-2004_10 |