HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium 1-tert-butyl tetrazole-5-thiolate → HCID 67606045, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium 1-tert-butyl tetrazole-5-thiolate | HCID 44598020 | — |
| Edukt | 2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-6-(chloromethyl)-2,2-dimethyl-1,3-dioxan-4-yl)acetate | HCID 67607702 | — |
| Produkt | HCID 67606045 | HCID 67606045 | — |
Reaktionsschritte
The procedure was carried out in the same manner as in Example 11, except that sodium 1-tert-butyl tetrazole-5-thiolate (3.6 g) prepared in Example 8 was used in place of sodium 1-phenyl-1H-tetrazole-5-thiolate, and 3.5 g of 2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-6-(chloromethyl)-2,2-dimethyl-1,3-dioxan-4-yl)acetate was used in place of 30 g thereof. The title compound was obtained (4.6 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08524914B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-abc27bb531384fe695337607a40f3259 |
| Quellennotiz | uspto-grants-2013_09 |