HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 22648201, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | N-Piperidinoethanol | HCID 18232 | — |
| Reactant | HCID 22648136 | HCID 22648136 | — |
| Solvent | ethyl N-ethoxycarbonyliminocarbamate | HCID 220568 | — |
| Product | HCID 22648201 | HCID 22648201 | — |
Reaction Steps
The title compound was prepared from 7 mg of 5-(2-chlorophenyl)-1-(2,6-dichlorophenyl)-7-hydroxy-3-methyl-3,4-dihydroquinolin-2(1H)-one, 40 mg of Ph3P, 20 μL of 1-piperidine ethanol, and 20 μL of diethyl azodicarboxylate by a procedure analogous to that described in EXAMPLE 2. Mass spectrum (ESI) 545 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06809199B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-b7cea77af76b4ca9a84e58332ea799c1 |
| Source note | uspto-grants-2004_10 |