HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethylhexyl acrylate → HCID 22034350, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethylhexyl acrylate | HCID 7636 | — |
| Reactant | 2-Ethylhexanoic Acid | HCID 8697 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 22034350 | HCID 22034350 | 99% |
Reaction Steps
A procedure similar to that of Example 2 was used for the reaction with 2-EHA. Starting from the TAIT product described in the preceding paragraph (1.0 g, ca. 4.5 mmol), 2-ethylhexyl acrylate (0.82 g, 4.5 mmol) and cesium carbonate (0.75 g, 2.25 mmol) in acetonitrile (20 mL), the product was isolated as a yellow oil and solid mixture (1.8 g, 99 %). IR: 3325, 2933, 2860, 1732, 1480 cm−1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06602831B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-86a0ae01e9da48f097884670e8dd499c |
| Source note | uspto-grants-2003_08 |