Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 86759096 | HCID 86759096 | — |
| Product | HCID 18176619 | HCID 18176619 | — |
Reaction Steps
Compound 74 (180 mg, 0.363 mmol) and morpholine (˜1 mL) were combined under Argon and heated to 80° C. for 2 h. Purification by flash column chromatography (hexane ethyl acetate 50:50) gave Compound 75 as an oil: 104 mg (0.240 mmol, 66%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06602872B1 |
|---|
| Source dataset | uspto-grants-2003_08 |
|---|
| ORD ID | ord-04e1d7fcdd00408cb29f906af1ab0206 |
|---|
| Source note | uspto-grants-2003_08 |
|---|
