HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3'-Hydroxyphenyl)propionic acid → Methyl 3-(3-hydroxyphenyl)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3'-Hydroxyphenyl)propionic acid | HCID 91 | — |
| Reactant | Methanol | HCID 887 | — |
| Catalyst | Sulfuric Acid | HCID 1118 | — |
| Product | Methyl 3-(3-hydroxyphenyl)propionate | HCID 1512675 | — |
Reaction Steps
1 g of 3-hydroxy-benzenepropanoic acid is mixed in 20 ml of methanol and 8 drops of sulphuric acid, the reaction medium is taken to reflux for 2 hours then evaporated under reduced pressure and purified by chromatography eluting with an AcOEt/Cyclohexane mixture 50/50. 1.07 g of expected product is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06602878B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-888b80259c3e4369881159b86a938bfc |
| Source note | uspto-grants-2003_08 |