HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 18177044, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Iodoheptane | HCID 20274 | — |
| Reactant | Piperidin-4-ol | HCID 79341 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18177044 | HCID 18177044 | — |
Reaction Steps
4-Hydroxypiperidine was dissolved in N,N-dimethylformamide (20 ml) and treated with potassium carbonate (1.5 g, 10.8 mmol) and 1-iodoheptane (1.8 ml, 11.3 mmol). After stirring for 2 h the mixture was diluted with ethyl acetate, washed with water, brine, dried and evaporated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06602882B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-4185a8181a894963a00059057df25bf8 |
| Source note | uspto-grants-2003_08 |