Fumarate → HCID 9869950, compound

Participants

Reaction Steps

Yield 0.9 g of 1-(4-fluorophenyl)-5-(2-methyltetrazol-5-yl)-3-[1-[2-(1-methyltetrazol-5-yl)-ethyl]-1,2,3,6-tetrahydropyridin-4-yl]-1H-indole, fumarate (17b). Mp 171-173° C. (ethanol). 1H NMR (DMSO-d6): δ 2.55-2.65 (m, 4H), 2.80 (t, 2H), 2.90 (t, 2H), 3.15 (t, 2H), 3.30 (broad s, 2H), 4.05 (s, 3H), 4.45 (s, 3H), 6.25 (broad s, 1H), 6.60 (s, 2H), 7.45 (t, 2H), 7.60-7.70 (m, 3H), 7.80 (s, 1H), 7.90 (d, 1H), 8.60 (s, 1H); MS m/z (%): 485 (MH+, 35), 346 (27), 140 (100).

Provenance & Evidence