HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 173244433, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Zinc Acetate | HCID 11192 | — |
| Reactant | HCID 173244476 | HCID 173244476 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 173244433 | HCID 173244433 | 95% |
Reaction Steps
A starting compound (9)(14.0 mg, 22.8 μmol) was dissolved in 1 mL of chloroform. A saturated methanol solution of zinc acetate (0.3 mL) was added thereto and stirred at room temperature for 30 minutes. The chloroform solution was washed with water and solvent was removed by distillation. As a result, the compound (10) (14.6 mg) was obtained in a yield of 95%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06602998B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-c03876ca1fd44c9b940facc3e7b7b26d |
| Source note | uspto-grants-2003_08 |