HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 17812156, compound → HCID 22313831, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 17812156 | HCID 17812156 | — |
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Product | HCID 22313831 | HCID 22313831 | 92.1% |
Reaction Steps
5-(5-(3-Fluoro-4-(1,3-thiazol-5-yl)phenyl)-3-trifluoromethyl-1H-pyrazol-1-yl)-2-pyridinesulfonamide (236 mg, 0.50 mmol) was dissolved with HCl—MeOH and the solvent was removed. The residue was washed with ethyl acetate to afford 233 mg (92.1%) of the titled compound as a slight yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06603008B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-ee48211e1c204b358e7500515897b415 |
| Source note | uspto-grants-2003_08 |