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HRID395407

反应详情

EQUATION

反应方程式

HRID 395407 的结构方程式

REACTANTS

反应物

2
结构：[I-].[Na+]
HCID5238

Sodium Iodide

INa

结构：COC(=O)c1c(C(F)F)nc(C(F)(F)F)c(CCl)c1CC(C)C
HCID22668817

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1c(C(F)F)nc(C(F)(F)F)c(CI)c1CC(C)C
HCID22668889

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

Reaction of methyl 2-(difluoromethyl)-5-(chloromethyl)-4-(2-methylpropyl)-6-(trifluoromethyl)-3-pyridine-carboxylate (U.S. Pat. No. 5,169,432 example 3) with sodium iodide in refluxing acetone according to the procedure known to those in the art yielded the product.

WORKUP

后处理

  1. customyielded the product