HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 18175008, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 18175046 | HCID 18175046 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18175008 | HCID 18175008 | — |
Reaction Steps
0.8 mmol of the compound obtained in Step B is dissolved in 10 ml of CH2Cl2 and then 1.2 mmol of triethylamine are added. The mixture is cooled with the aid of an ice bath and 1.2 mmol of ammonium hydroxide solution are added dropwise. After stirring for 2 hours, the mixture is evaporated and the residue obtained is recrystallised.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06605632B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-49b40a4fb0d3447491c8b53f5e7ccd68 |
| Source note | uspto-grants-2003_08 |