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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 395583Generated: October 29, 2026

Thionyl Chloride → HCID 18175096, compound

https://huagongshe.com/reaction/395583

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThionyl ChlorideHCID 24386—
ReactantHCID 18175064HCID 18175064—
ProductHCID 18175096HCID 18175096—

Reaction Conditions

Temperature60 °C

Reaction Steps

The product obtained in Step A (3 mmol), dissolved in thionyl chloride, is stirred at 60° C. under a current of nitrogen for one hour. The thionyl chloride is evaporated off under reduced pressure and the residue is dried with the aid of a vane pump to yield the title product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06605632B1
Source datasetuspto-grants-2003_08
ORD IDord-e85f8cd54ef74a9f81c35d4c7f125d74
Source noteuspto-grants-2003_08