HCID 86590365, compound → HCID 10179984, compound

Participants

Reaction Steps

8-[5-(3-Dimethylamino-propylidene)-tricyclo[2.2.1.02,6]hept-3-yl]-1,3-dipropyl-3,7-dihydro-purine-2,6-dione; compound with trifluoro-acetic acid was hydrogenated under 60 psi using Pt/C 5% in EtOH (10 ml) and 1 ml conc. HCl overnight. Catalyst was filtered and solvent was removed under reduced pressure. Crude product was purified by HPLC Yield 30 mg. Mass (ES+ 414).

Provenance & Evidence