HCID 18173027, compound → HCID 18173037, compound

HRID 395879Notes

Reaction equation

HRID 395879 reaction equation
[O:1]=[C:2]1[N:10]([CH2:11][CH2:12][CH3:13])[C:9]2[N:8]=[C:7]([C:14]3[CH2:20][CH:19]4[CH:21]([C:22]([OH:24])=[O:23])[CH:16]([CH2:17][CH2:18]4)[CH:15]=3)[NH:6][C:5]=2[C:4](=[O:25])[N:3]1[CH2:26][CH2:27][CH3:28]>C(OCC)(=O)C.[Pd]>[O:1]=[C:2]1[N:10]([CH2:11][CH2:12][CH3:13])[C:9]2[N:8]=[C:7]([CH:14]3[CH2:20][CH:19]4[CH:21]([C:22]([OH:24])=[O:23])[CH:16]([CH2:17][CH2:18]4)[CH2:15]3)[NH:6][C:5]=2[C:4](=[O:25])[N:3]1[CH2:26][CH2:27][CH3:28]

Participants

4

Reactant 1

HCID 18173027HCID 18173027, compound

Product 1

HCID 18173037HCID 18173037, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 8857Ethyl AcetateSolvent

Procedure

3-(2,6-Dioxo-1,3-dipropyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-bicyclo[3.2.1]oct-2-ene-8-carboxylic acid (Example 29) was hydrogenated using Pd/C in ethyl acetate. Mass (ES+ 389).

Sources & evidence

ORD record
ord-432d3be51eb749dcba27978787618dac
Source dataset
uspto-grants-2003_08
Patent number
US06605600B1

Reaction notes

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