HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 10155447, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 18173103 | HCID 18173103 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10155447 | HCID 10155447 | — |
Reaction Steps
8-(8-Oxo-bicyclo[3.2.1]oct-3-yl)-1,3-dipropyl-3,7-dihydro-purine-2,6-dione (25 mg) was reduced using NaBH4 (30 mg) in MeOH at 0° C. The product was purified by HPLC. Yield (7 mg). Mass (ES+ 361).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06605600B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-8d0b19adc88949aea9be93de95a92d38 |
| Source note | uspto-grants-2003_08 |